must

This week I cover mead making fermentation and finishing. Last week in part 1, I provided an overview of mead making and the first steps of making the must, pitching your yeast and adding nutrients. This week I will cover the remaining steps. As I covered last week the key components of modern mead making […]
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In August 2020, the federal Food & Drug Administration (FDA) finalized the definition and labeling requirements of gluten-free fermented and hydrolyzed foods (including beer and other alcoholic beverages).  The ruling provides a clear delineation between products that are truly gluten-free and products that are not and how product labels communicate those differences to consumers.  In […]

The post Gluten-Free Brewers Group Responds to FDA Final Rule on Gluten-Free Claims on Fermented Foods appeared first on CraftBeer.com.

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Brewers often joke that they spend more time cleaning than on any other aspect of the job. That isn't quite true at Sapwood Cellars, but the cleaning aspect has been the biggest change from homebrewing. By comparison, wort production hasn't been that difficult or different. Sure it took a few batches to acclimate to the efficiency and losses on our 10 bbl Forgeworks brewhouse (as with any new brewing system), made more challenging by an unreliable flow meter. Even 15 batches in despite hitting our target mash temps, wort fermentability seems to be lower than expected. We're also still dialing in hop utilization given the thermodynamics involved with large wort volumes. Still, the concepts, ingredients, and techniques are all pretty similar to homebrewing.

When it comes to cleaning and sanitizing though, we've had to relearn the entire process. You really can't fill a fermentor with 360 gallon of Oxiclean Free and soak overnight or swirl and scrub... I miss those days. First, let's talk about chemicals and what they do. Our main supplier is AFCO, but Berko, Five-Star, and Loeffler all have fans. Prices seemed similar, we just didn't think about ordering until a couple weeks before we started brewing and picked the one with the quickest turnaround time. We buy most of the chemicals in 5 gallon jugs, and pump them into beakers to measure and dose.

The chemicals we use to clean and sanitize our brewery.

Chemicals

Caustic (5229 Caustic) - Caustic is the primary cleaner used by most breweries. Usually sodium hydroxide based and heavily alkaline. It is ideal for breaking down and removing organic deposits (e.g., krausen rings). You can do a bit of trading-off between time, temperature, pressure, and concentration. That said, 2-3% caustic at ~150F (66C) for 20-30 minutes through the sprayball has been a pretty good place to start for us. Caustic is dangerous because it is capable of breaking down your skin (the lye used in soap making is similar). We started with a powdered caustic (Wash-It), but given the price and efficacy we transitioned to liquid.

Phosphoric-Nitric Acid Blend (5397 Microlex Special 30) - Acid helps to remove inorganic deposits, i.e., beerstone (calcium oxalate). It also helps to neutralize any residual caustic (not that there should be any with adequate rinsing) and to passivate stainless steel. Acid blend is used at similar temperatures and cycle lengths as caustic, although slightly cooler, ~130F (54C).

Five Star Peroxyacetic Acid (PAA) - While there are many sanitizers available, PAA is the most popular for breweries. At the right concentrations it is a robust sanitizer with high effectiveness. It breaks down to acetic acid, so it can be used no-rinse. It is a powerful oxidizer, which makes it important to drain any residual before fermented beer enters a tank or keg. Our bucket was leftover from the old brewery in our space, so we bought a pack of test strips and it still reads the expected concentration after dilution.

Five Star PBW - We have a bucket of this alkaline powered cleaner for soaking hot-side equipment and other gear where we don't want to have to be as careful as we would with caustic. We both used it at home, so were more comfortable with it than the Chlorinated Manual Cleaner we started with.

Iodophor (4330 Spark I2) - Similar to the PBW, it is nice to have a less hazardous sanitizer for spraying ports or soaking fittings. It is only effective on clean surfaces, so it is important to remove of detritus before expecting it to work.

Grain Alcohol - Given its quick kill times and evaporation ethanol is the ideal sanitizer for spray bottles and any surfaces that are highly sensitive (e.g., yeast culturing). Isopropyl alcohol is another option.

General Concepts

Pre-Heating - At this scale a tank has so much thermal mass that you can't simply put 15 gallons (57 L) of hot water to a tank and expect it to still be hot after circulating. As a result if you want the caustic or acid to stay hot, you need to pray hot water into the tank. A tank with an electric element (like our keg washer has) helps too.

Sprayball - Most tanks have a port that leads to a sprayball, a small metal orb that spins and sprays when liquid is forced through. These aren't always perfect, and can have blind spots, especially in ports and above it. In addition, it isn't effective at cleaning its own exterior.

A sprayball from our kettle.

Passivation - This is what makes stainless steel stainless, a thin layer of chromium atoms at the surface that prevents iron from rusting or leeching into the beer (which weakens the equipment and shortens its lifespan). With a pristinely clean surface, the oxygen in the atmosphere is enough to accomplish this, but acids (especially nitric) are more effective.

Safety

These chemicals aren't anything to joke about. Many brewers have scars gained from caustic or acid dripping onto their skin . Safety glasses, long gloves, chemical resistant boots and pants are a must when handling them. Read the safety data sheet for each chemical you are using and know what to do if some gets on your skin or in your eyes. I don't get to drink as much beer as I used to because the end of the day is usually the most dangerous time.

Scott and I prefer to have all of the tank's arms connected from the start, allowing us to use valves to direct the flow of the cleaning and sanitizing solutions. We started off using a manifold coming off the pump, but have changed to daisy-chained T's between the arms. Many brewers prefer to simply move a single output line from the pump between the arms. This requires less setup time, but more active effort once cleaning begins (moving the hose from arm to arm ~10 times through the process). It also carries additional risks if you move the hose without closing a valve.

Our Fermentor CIP Process

1. Once the beer is out of a tank, we turn off the glycol jackets and open the dump valve. We then shoot high-pressure cold water through the sprayball to remove most of the hops/yeast struck to the sides and bottom.

2. We use our on-demand hot water heater to generate 130F (54C) water to spray through the sprayball and manually through a hose to dislodge the bulk of the crud stuck to the sides/top of the fermentor. We'll run it through the pump to get good coverage.

Tankless on-demand hot water heater.

3. We briefly remove the lower fittings on the tanks (including manway, racking arm, thermometer, sample port) to spray out the trub caught in them.

4. We blow compressed air through the sprayball at ~30 PSI with the bottom valve open for 30 minutes. CO2 neutralizes caustic, so best to remove as much as possible before proceeding. This long is likely overkill for a 10 bbl tank, but can't hurt.

5. We assemble our cleaning rig, usually a pump running to the sprayball, with a T to connect it to the racking arm and another to the blow-off.

The pump we use for cleaning.

The fermentor during the cleaning process.

5. We preheat the tank for a couple minutes by spraying 160F (71C) water in and letting it drain. We hook the water line in right before the pump so we can immediately go to cleaning once it is preheated. Our goal is to get the tank to read ~130F (54C).

6. We then use the hot water heater's built-in meter to send 10-15 gallons of 160F (71C) water into the tank. We dose in 3 oz of caustic per gallon (2.3%) using a stainless steel elbow on one of the ports (chasing the caustic with water to ensure it get in). We then turn the elbow down to allow that port to equalize the pressure inside the tank, while preventing caustic from spitting out.

7. I like to send a little flow through the blow-off and racking arm first to soak them during the 20-25 minutes sprayball at full pressure (60 hz on our pump - or a bit slower if it cavitates). Then five minutes through the other arms, before a final five through the sprayball.

6. Dump the caustic. Rinse each arm with hot water, then burst rinse 10 times for 10 seconds at 130F (54C) through the sprayball, allowing it to drain before each successive rinse. I'll often put 10-15 gallons (38-57 L) into the tank once or twice and recirculate at the end to make sure there is enough pressure to spray all the surfaces. You can check the pH of the drained rinse water to ensure it has returned close normal before proceeding.

2. We then take off all of the fittings (including the sprayball itself), soak them in PBW or caustic. We inspect the fittings and gaskets, rinse and put into a bucket of iodophor. For the ports we spray, scrub and spritz with iodophor before reassembling. We also take the chance to inspect the interior with a flashlight to ensure there are no deposits.

7. We run acid blend at 2 oz per gallon (1.5% by volume) using roughly the same process and times as the caustic. Significantly higher concentrations should be used on new equipment and once a year to ensure adequate passivation.

8. Usually we'll air-dry at this point unless we need the tank the following day. In that case we'll rinse and then sanitize with peroxyacetic acid in cool water at 200 PPM using the same rig, and pressurize the tank to 4 PSI of CO2 to ensure it holds. The next morning we'll dump any residual sanitizer from each port before running wort or beer in.

The whole process including sanitation takes three hours, but most of that time isn't active (just waiting for a purge, or cycle). Going longer on any of the times isn't a big deal, so it is easy to run while working on other things if you keep track of your progress and don't miss a step.

We haven't gotten a CIP cart with dedicated vessels and pump, so our biggest issue currently is that it is difficult for one of us to clean a tank while the other person brews because they require some of the same equipment. Luckily our current schedule of two batches a week doesn't make that too much of an issue.

I am by no means holding this up as a perfect or ideal process. It'll likely be viewed as overkill by some, and inadequate by others. But if you have constructive suggestions, I'd love to hear them! I'd rather err towards overkill because we're dealing with several yeast strains (including killer wine yeast, Saccharomyces cerevisiae var. diastaticus, not to mention Brettanomyces and Pediococcus in a dedicated tank), although we do have the advantage of only dealing with kegs stored cold.

Other Pieces

We addition we'll pump the same chemicals through our heat exchanger and carbonation stone. For the heat exchanger we also heat pasteurize by running 180F (82C) water for 20 minutes inline once we assemble our knock-out rig (we discard the water until we see wort before sending to the fermentor). Our keg cleaner automatically does the same process on our sanke kegs, including air and CO2 purges to recapture the caustic and sanitizer.
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I've brewed a surprising number of beers with ingredients grown on our .1 acres of Washington, DC. Including hops, cherries, juniper, ground ivy, mulberries... and recently fermented acorns! Rather than showcase a single ingredient though, I wanted to brew an estate beer with five ingredients grown and harvested on our land!

Aged homegrown Cascade hops in the boil.

The extent of the influence of aged hops on sour beer is still a bit underestimated. While the generally stated goal is preventing rapid souring by Lactobacillus in a traditionally fermented lambic, what they add to the flavor and what particular characteristics of the hops best serve this isn't widely studied. There are a few studies that oxidation can boost certain fruity aromatics. Which has lead Scott to threaten to use old hops on the hot-side for a NEIPA... he promised to do a test batch before brewing a 10 bbl batch on the new Sapwood Cellars brewhouse.

I thought it would be fun to brew with aged Cascades from the bines in my backyard, especially because fresh they didn't have a huge aroma. They'd been sitting open in my basement since they were dried a few years before. 

Flour slurry pouring in.

I don't have the space or effort to grow or malt grain, so I took the easy way out and brewed with wheat malt extract (a blend of 65% wheat malt 35% barley). I'd had good results from extract lambics previously, but this time in addition to maltodextrin I added wheat flour slurry to the boil. Mixing the flour with cold water prevents it from clumping when it touches the boiling wort. A turbid mash pulls starch from the unmalted wheat into the boil, which eventually feeds the various microbes in the late-stages of fermentation. The microbes must have enjoyed it as the resulting beers are completely clear.

All of the frozen berries (cherries, blackberries, raspberries, and mulberries.

Fruit was provided by our four berry trees/bushes. Sour cherry, blackberry, raspberry, and mulberry. To keep things easy I added roughly equal amount of each (other than the raspberries). I briefly froze most of the fruit, but I added the raspberries a small handful at a time as they ripen slower than the rest. I only had enough of each for one gallon of beer, as most of the rest of the fruit was spoken for. The leftover beer went onto local plums!

Video Review



Backyard Berries

Smell – Cherry and raspberry lead, not surprising as they are more distinct than the blackberry and mulberry. There is an underlining wine-iness that likely comes from the rest of the fruit. The base beer behind the fruit doesn't make itself known other than a subtle maltiness.

Appearance – Clear garnet on the first pour, a little haze when I emptied the bottle into the glass. Alright head retention thanks to the wheat.

Taste – Reminds of the nose with raspberry up front and cherry jam into the finish. Not as bright and fresh as it once was, but still reasonably fresh. The malt and hops don’t add a huge amount of character, but they support the fruit. The Wyeast lambic blend similarly stays mostly out of the way, adding edge complexity without trying to fight through the fruit.

Mouthfeel – Not a thick beer given the relatively low OG, and all of the simple sugars from the fruit. Solid carbonation, CBC-1 did a good job despite the acidity.

Drinkability & Notes – The combination of four berries works surprisingly well to my palate. They play together without becoming generic fruitiness. The base beer is unremarkable, but that’s fine in a beer where the fruit is the star.

Changes for Next Time – Would be nice to brew more than a gallon, but otherwise my only real changes would be to go all-grain.

The finished mixed-berry sour beer.

Plum-Bus

The rest of the batch went onto a two varieties of local plums. I've brewed with plums before in a dubbel. I wasn't sure about plums in a pale beer, but after trying spectacular examples from Tilquin and Casey I was convinced!

Smell – Clear it isn’t a kettle-soured fruit-bomb, lots of lemon pith and mineral along with the moderate fruit contribution. Plums aren’t nearly as aromatic as the more common sour beer fruits, but they add a depth without covering up the base beer.

Appearance – Beer is more rusty-gold than purple. Clear despite the flour. Thin white head, but this bottle appears less carbonated than the last few I’ve opened.

Plum sour beer.

Taste – Tangy plum skin, apricot, and lemon. Beautiful blend of fruit and beer. Wyeast Lambic Blend with dreg-augmentation again does a really nice job. Strong lactic acid without any vinegar or nail polish. Finish is moderate funk, hay, and overripe stone fruit.

Mouthfeel – Light, but not thin. Carbonation is too low, maybe the cap-job on this one wasn’t perfect.

Drinkability & Notes – Delicious. The plum could be a little juicier and fresher, but it works well. Sad I didn’t leave any of this half unfruited for comparison.

Changes for Next Time – I’d like to keep experimenting with other plum varieties in beer. Glad the pale base worked out well. Despite “plum” being a common descriptor for darker Belgians, actual plums don’t shine with all of that malt.

Defrosting plums in a 3 gallon Better Bottle.

Recipe

Batch Size: 10.00 gal
SRM: 5.5
IBU: 5.3
OG: 1.046
FG: 1.006/1.006
ABV: 5.25%
Final pH: 3.45/3.45
Boil Time: 90 mins

Fermentables
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92.3% - 9 lbs Breiss Bavarian Wheat DME
5.1% - .5 lbs Maltodextrin Powder
2.6% - .25 lbs King Arthur All Purpose Flour

Hops
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2.50 oz - Homegrown Cascade: Aged 3-4 Years (Whole, ~1.00% AA) @ 90 min

Yeast
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Wyeast Belgian Lambic Blend
or
Omega OYL-218 - All The Bretts
Omega OYL-057 - HotHead Ale

Notes
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Brewed 1/15/17

Hops were homegrown and aged open over several years.

Fermented and aged in 6 gallon BetterBottle without transfering. Added some various dregs over the course of fermentation.

7/21/17 Filled a 1 gallon jug with the Wyeast half onto 6 oz each homegrown sour cherries, blackberries, and mulberries (plus maybe an ounce of raspberries - maybe 4 oz total over a couple months). The remainder went onto 3 lbs of methly plums.

8/24/17 Added an additional 1.75 lbs of Castleton plums to the plum portion

12/14/17 Bottled the 2.75 gallons of the plum with 61 g of table sugar and rehydrated CBC-1. Bottled the .8 gallons of backyard fruit with 21 g of table sugar and CBC-1.

All the fruit growing in my backyard!
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